MATERIAL ANALYSIS

Material analysis techniques: which one for which need

The question is almost never "which technique". It is "what do I need to know about this material". The acronyms come afterwards — and one of them answers, while the others cost a lot for nothing.

7 techniques
Compared on what they read
The question first
The acronym after
The whole chain
From the instrument to the campaign

The seven techniques, and what each one reads

The acronym on the left, the question it answers on the right.

X-ray fluorescence — XRF Which elements and in what quantity. On site, in seconds, destroying nothing. Does not read light elements.
Raman Which molecule, which polymer, which pigment. Through a vial or a bag, without contact.
Infrared — FTIR The chemical functions of a plastic, an oil, a binder. Complementary to Raman more than competing with it.
Electron microscopy and EDX — SEM/EDS Seeing the structure at the micron, then analysing precisely the spot being looked at.
X-ray diffraction — XRD Which crystalline phase. Two powders of the same composition can be two different materials.
X-ray photoelectrons — XPS The very first nanometres of the surface, and the chemical state of the elements found there.
Spark — OES Carbon and light elements in metals — precisely what escapes X-ray fluorescence.

Start from your question

Six common questions, and the technique that answers each.

"Which elements, and how much?"

X-ray fluorescence. The fastest and cheapest answer when the question is elemental — and it often is.

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"Which molecule, which plastic?"

Raman, or infrared. Elemental analysis cannot tell apart two polymers made of the same atoms: the bond has to be read.

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"What exactly is at this spot?"

Electron microscopy and EDX. When the defect is a few microns across and has to be seen before it can be analysed.

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"Which phase, not just which elements?"

X-ray diffraction. Graphite and diamond are the same element. Only the structure tells them apart.

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"What is happening at the surface?"

XPS for the first nanometres and the chemical state; X-ray fluorescence for the thickness of a deposit.

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"Does carbon decide my grade?"

Then X-ray fluorescence will not be enough: it takes spark, on the floor or in the laboratory.

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Interfaçage de Raman dans un microscope électronique à balayage

The techniques do not compete, they follow on from each other

In practice a question is rarely settled in one move. You look under the microscope, analyse the spot you looked at, then confirm the chemical nature by another route. Some set-ups do both in the same instrument — a Raman built into an electron microscope, for one.

Depending on the case, we equip your teams or run the campaign ourselves. The question asked decides the set-up, and we cover both.

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Tell us what you are trying to find out

Describe the sample and the decision that depends on the result. We will tell you which technique answers, and how to get it: instrument, measurement campaign, or both.